Laboratory time-resolved X-ray diffractometry for <i>in situ</i> studies of crystalline materials under uniaxial compression and vibration
نویسندگان
چکیده
A novel laboratory diffractometer for time-resolved high-resolution X-ray diffraction studies of reversible and irreversible processes in crystalline materials under uniaxial compression vibration is described. Temporal resolution up to milliseconds double-crystal tens seconds triple-crystal experiments was achieved with a single adaptive bending optics element. Design solutions techniques applying controlling situ are Results presented various static dynamic load experiments, controlled by system based on the TANGO Controls framework. Rocking curves paratellurite (TeO 2 ) quasi-static lithium fluoride (LiF) ultrasonic were measured temporal resolution. Reciprocal-space maps LiF quartz (SiO collected.
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ژورنال
عنوان ژورنال: Journal of Applied Crystallography
سال: 2022
ISSN: ['1600-5767', '0021-8898']
DOI: https://doi.org/10.1107/s160057672101236x